Illya, recuperating in the hospital, is kidnapped by an old enemy, Viktor Karmak, to lure Solo into a trap. Solo follows a clue to a twelve block condemned area of Manhattan, and finds modern artist Sheila Van Tillson. Karmak appears and announces that Solo has until dawn to find Illya before a deadly gas kills him, while Karmak and his pet jaguar will try to hunt Solo down at the same time.
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 Robert Vaughn |
Napoleon Solo |
 David McCallum |
Illya Kuryakin (1964-1968) |
 Leo G. Carroll |
Alexander Waverly |
 Darren McGavin |
Viktor Karmak |
Guest Star |
Marlyn Mason |
Sheila Van Tillson |
Guest Star |
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